Volume 17 Issue 7

Published: 2025-06-25

Contents


Article
Application of Trifluoperazine Hydrochloride as a Chromogenic Reagent for Spectrophotometric Determination of Sulphacetamide Sodium – Application to Ophthalmic Preparations

Raeeid M. Kadder, Nabeel S. Othman,

A simple, rapid and sensitive spectrophotometric method for the determination of sulphacetamide sodium (SAS) was described. The method based on the oxidative coupling reaction of trifluoperazine...

DOI: 10.33899/rjs.2006.43679

Pages: 92-103
Study of Charge Transfer Complexes of Salicylideneanilines and its Substituents with Pr(fod)3 in Cyclohexane by U.V. Spectroscopy

May G. Al-Dabbagh, Layla M. Saleem,

Salicylidene aniline and its substituents form 1:1 charge transfer complexes with the lanthanide shift reagent Pr(fod)3 in cyclohexane indicated by the observation of a new band in their U.V....

DOI: 10.33899/rjs.2006.43663

Pages: 59-67
Isolation and Identification of a Pigment from Grape for Use as Acid-Base Indicator.

Diar S. Ali, Kamal M. Mahmoud,

This paper deals with the extraction of a pigment (Malvidin-3-fructoside) from the Iraqi Kurdistan grape (Vitis vinifera L.). The extracted pigment was purified using physical methods including...

DOI: 10.33899/rjs.2006.43716

Pages: 121-133
Synthesis of Some New 2-(2-Isopropyl-5-Methyl Phenoxymethyl)-5-Aryl-1,3,4-Oxadiazoles

Said A. Said,

In the present investigation, some new 1,3,4-oxadiazole derivatives have been prepared starting from readily available thymol. The reaction of thymol with ethylbromoacetate afforded the ethyl ester...

DOI: 10.33899/rjs.2006.43660

Pages: 52-58
Preparation and Study of Some Effects of γ – Radiation on Some New Copper(II) Complexes Containing Mixed Ligands; Substituted Salicylic Acid and Benzoin semicarbazone

Younis T. Mahmood, Zuhoor F. Dawood,

Complexes of the type [Cu(B`SCH)(AH)](NO3)2 and [Cu(B`SC)(A)] have been prepared in neutral and basic mediam, respectively, (where AH= substituted salicylic acid: salicylic acid-SA and...

DOI: 10.33899/rjs.2006.43631

Pages: 1-14
Histidine as a New Coupling Agent for The Spectrophotometric Assay of Sulphadiazine – Application to Pharmaceutical Preparations

Raeeid M. Kadder, Nabeel S. Othman,

A simple and sensitive spectrophotometric method for the assay of sulphadiazine (SDA) in aqueous medium is described, the method is based on the formation of a yellow coloured azo dye from the...

DOI: 10.33899/rjs.2006.43648

Pages: 25-35
Square Wave Voltammetry Determination of Coenzyme Q10

timad I. Taha, Sadallah T. Sulaiman, Haitham A. AL-Wahab,

An easy and extremely sensitive square wave voltammetric method for the determination of coenzyme Q10 has been evolved. The method is based on the direct measurement of the reduction peak current...

DOI: 10.33899/rjs.2006.43674

Pages: 86-91
Synthesis of Some New Fused Heterocyclic Rings Derived from 3-Benzofuranone

Mohammad A. Eisa,

In the present work, the synthesis of some new fused heterocyclic rings derived from 3-benzofuranone was achieved. 3-Benzofuranone (1) was prepared by the action of polyphosphoric acid on...

DOI: 10.33899/rjs.2006.43670

Pages: 76-85
Electrical Conductivity of [Co(en)2Cl2] Cl in Mixed Solvents (Alcohol + Water) at 298K

Shatha M. Quba, Amel G. Abed, Banan A. Akrawi,

The electrical conductivity of trans dichloro bis(ethylenediamine) cobalt (III) chloride [Co(en)2Cl2] Cl has been measured in (methanol + water), (ethanol + water) and (isoproponal + water) at...

DOI: 10.33899/rjs.2006.43713

Pages: 104-120
Chemical Analysis of Gastric Juice in Duodenal Ulcer Patients Infected with Helicobacter Pylori

Layla A. Moustafa,

The research was concerned with chemical analysis of the gastric juice in duodenal ulcer patients caused by Helicobacter pylori infection. The study included (25) patients (13 males and 12 females)...

DOI: 10.33899/rjs.2006.43657

Pages: 45-51
Multinuclear Complexes of Co+2,Ni+2,Cu+2 and Sn+2With (o,o′-Diethyl Dithiophosphate)Tin(IV)

Einas H. Mohamed, Nabeel H. Buttrus,

Tin metal react with bis (thiophosphoryl) disulfide in refluxing toluene to give the compound tetrakis- (o,o-diethyl dithiophosphate) tin(IV). [Sn{S2P(EtO)2}4], through an oxidative addition...

DOI: 10.33899/rjs.2006.43645

Pages: 15-24
The Electrical Conductivity of Potasium Halides in Methanol at Different Temperatures

Ashur M. Dawod, Salem M. Khalil, Banan A. Akrawi,

In the present study we have measured the electrical conductivity of some potassium halides (KCl, KBr and KI) in methanol at different temperatures (298-318K). The conductivity parameters (R, Ka...

DOI: 10.33899/rjs.2006.43667

Pages: 68-75
Synthesis and Biological Activity Study of Some New Substituted Pyrrolidines

Rana A. AL-Obaidy, Abdul-Wahab J. AL-Hamdany,

Chalcones (1,3-diaryl-2-propen-1-ones) (1-13) were prepared using Claisen-Schmidt condensation, while Schiff bases (N-arylidene benzylamines) (14-20) were produced by the condensation of benzyl...

DOI: 10.33899/rjs.2006.43651

Pages: 36-44